Other Test Method (OTM)-50 data for fluorinated volatile compounds in the emissions from air pollution controls at a fluoropolymer manufacturer. This dataset is associated with the following publication: Shields, E., W. Roberson, J. Ryan, and S. Jackson. The Use of Air Pollution Controls to Reduce the Gas-phase Emissions of Per- and Polyfluoroalkyl Substances from a Fluoropolymer Manufacturing Facility. Environmental Science & Technology Letters. American Chemical Society, Washington, DC, USA, 0, (2025).